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Flame Photometer (four elements: K, Na, Li, Ca)

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  • 产品名称:Flame Photometer (four elements: K, Na, Li, Ca)
  • 产品型号:FP6440
  • 产品展商:Shanghai Chi Tang
  • 产品文档:无相关文档
简单介绍

3. measurement elements: potassium, sodium, lithium, calcium;

产品描述

Detailed product

Product description

1. display mode: dual channel LCD liquid crystal display reading;

2. measuring element keyboard can be free to choose;

3. measuring elements: potassium, sodium, lithium, calcium;

The calibration of 4. curved I line: clearing method, straight line method;

5. measuring range: range adjustment: K:0-15 mu g/ml, 0-40 g/ml, 0-60 g/ml, 0-100 / g/ml; Na:0-40 g/ml, 0-80 g/ml, 0-120 g/ml, 0-160 / g/ml; Ba:0-3000 g/m; Li:0-100 g/ml; Ca:0-1000 g/ml
Working principle

Flame photometric method According to the Rome gold formula for quantitative analysis, i.e. B I=aXc, I line intensity of C, is the content of the measured elements, D is to be measured and elements of evaporation and excitation conditions related to B constant; self absorption coefficient, because with the flame as excitation light source, the temperature through the control of the air and gas flow to maintain stability, because of the use of liquid sample, less sample components, so in the determination of a is a constant, generally due to the sample concentration is low, the self absorption is negligible, so I= lambda C, and can be used to measure the relative intensity method analysis.

Flame Photometric analysis When the liquid used to import flame atomizer into sol, measured by thermal dissociation of generating elements Ground state atom In the flame, was inspired by the spectrum. Monochromator Into Monochromatic light After the photoelectric measurement system, the flame of the humidity is relatively low, therefore can only stimulate minority elements, and the spectrum is relatively simple, less interference, Flame photometric method Especially for more easily excited alkali metal and Alkaline-earth metal The determination.

In the determination, in order to stabilize the flame and eliminate the interference of some elements, often in the determination of liquid in the "buffer", such as K, Ca, Mg and between the determination of impact, if these three kinds of elements with saturated solution as "buffer", the solution to a certain amount, effect is generated is a single constant value, can be used for background subtraction, measurement of sodium, a large number of HCO32- can make the result is low, heating to remove hydrochloric acid solution available.

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influence factor

Lamp current

Flame atomic absorption spectrophotometer using light source are hollow cathode lamp, hollow cathode lamp has a lamp current operating parameters. The lamp current determines light radiation intensity. Increase the current headlights in a certain range can be increased at the same time, radiation intensity, light stability and the signal-to-noise ratio is also increased, but decreased the sensitivity of the instrument. If the lamp current is too large, will cause the lamp itself from the corrosion phenomenon and shorten the service life of the lamp; the discharge is not normal, the light radiation intensity is not stable. On the contrary, reducing the lamp current can reduce the radiation intensity in a certain range, the sensitivity increased, but the light stability and decreased signal-to-noise ratio. If the lamp current is too low, and can make the lamp radiation intensity, resulting in a serious decline in stability and the signal-to-noise ratio to be used. Therefore, in the detection of specific work, such as the measured sample concentration was higher than the current headlights use, in order to achieve good stability; as the tested samples of low concentration, while maintaining stability to meet the requirements of the premise, the use of the lamp current is low, in order to obtain better sensitivity.

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